Zhao Rixin, Lu Shuangfang, Xue Haitao, et al. Effect of SEM parameters on quantitative evaluation of shale micropores[J]. 2019, 40(5): 1141-1154.DOI: 10.11743/ogg20190520.
We studied the microscopic pore structure of the organic-rich Longmaxi Formation shale in Sichuan Basin through Argon Ion milling-Field Emission Scanning Electron Microscopy characterization with different SEM parameters
and investigated the effect of electron microscopic parameter variation on the quantitative evaluation of the microscopic pores of shale based on the pore data extracted by the "optimal threshold method" within the same field of view.The results show that the probe current and accelerating voltage among these electron microscopic parameters
have greater influence on the accuracy of quantitative pore data extraction.When the beam exceeds 170PA
the higher the voltage is adjusted to
the smaller the large pore area is extracted.When the voltage exceeds 15KV
the beam current is lower
and the pores extracted are relatively more complete; while as the beam current is lower than 86PA
the longer the scanning time is
the more completely the pore is extracted
but as it exceeds 86PA
the scanning time has little effect on pore extraction.In addition
luminance and contrast values of excessive lowness or highness are detrimental to pore extraction
and the pore extraction comes to the most complete when their values are 47.5 and 85 respectively.In conclusion
the parameters of electron microscopy have a remarkable influence on the extraction of organic pores
and the proper selection of parameters can significantly improve the accuracy of quantitative data extraction for shale micropores
in a bid to obtain more realistic data of shale micropore structure.